A simple Sonochemical route for synthesis silver selenide nanoparticles from SeCl۴ and silver salicylate; Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry

نویسندگانمریم جعفری رنانی-مسعود صلواتی-کمال صابریان-هومن صبارو
نشریهSYNTH REACT INORG M
تاریخ انتشار۲۰۱۵-۱۰-۰۱
نمایه نشریهISI

چکیده مقاله

For the first time, silver salicylate marked as [Ag(HSal)] was applied to fabricate silver selenide nanoparticles. This paper describes a simple approach based on reaction between silver salicylate as an inorganic precursor, SeCl4 and hydrazine hydrate (N2H4.H2O) via sonochemical route for the fabrication of silver selenide (Ag2Se) nanoparticles. The effect of preparation parameters such as pH, ultrasonic power, and reaction temperature on the morphology of the final products was investigated. Ag2Se nanoparticles were characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), and X-ray energy dispersive spectroscopy) EDS).