| نویسندگان | فاطمه سادات سنگ سفیدی-مهدیه اسمعیلی زارع-مسعود صلواتی |
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| نشریه | J IND ENG CHEM |
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| تاریخ انتشار | 2015-2-01 |
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| نمایه نشریه | ISI |
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چکیده مقاله
In
this
paper,
HgS
nanostructures
were
synthesized
from
the
reaction
of
N,N
0
-(disalicylidene-1,
4-diaminobutane)
mercury
complex,
[Hg(salbn)]
as
a
novel
precursor,
via
hydrothermal
method.
This
method
is
facile
and
provides
an
appropriate
condition
for
the
preparation
of
structures
with
various
morphologies.
In
this
study,
the
effect
of
different
parameters
such
as
type
of
sulfur
sources,
reaction
time
and
type
of
alkaline
source
on
the
morphology
and
the
particle
size
were
studied.
The
results
indicated
that
the
type
of
sulfur
source
plays
an
important
role
in
the
morphology
of
as-synthesized
HgS.
The
synthesized
materials
were
characterized
by
means
of
X-ray
diffraction,
transmission
electron
microscopy,
scanning
electron
microscopy,
infrared
spectrum
and
energy
dispersive
X-ray
analysis.
Flower-like
HgS
microcrystals
were
obtained
by
using
TGA
as
sulfur
source.
The
obtained
results
are
discussed
in
detail.
