نویسندگان | مصطفی زاهدی فرد-احسان صادقی-مزدیان فرد-الناز حبیبی |
---|---|
نشریه | Applied Radiation and Isotopes |
نوع مقاله | Full Paper |
تاریخ انتشار | August 2013 |
رتبه نشریه | علمی - پژوهشی |
نوع نشریه | چاپی |
کشور محل چاپ | ایالات متحدهٔ امریکا |
چکیده مقاله
Nanoparticles of cerium doped calcium fluoride (CaF2:Ce) were synthesized for the first time using the hydrothermal method. The formation of nanostructures was confirmed by X-ray diffraction (XRD) patterns, indicating cubic lattice structure for the particles produced. Their shape and size were observed by scanning electron microscopy (SEM). Thermoluminescence characteristics were studied by having the samples irradiated by gamma rays of 60Co source. The optimum thermal treatment of 400 °C for 30 min was found for the produced nanoparticles. The Tm−Tstop and computerized glow curve deconvolution (CGCD) methods, used to determine the number of component glow peaks and kinetic parameters, indicated seven overlapping glow peaks on the TL glow curve at approximately 394, 411, 425, 445, 556, 594 and 632 K. A linear dose response of up to 2000 Gy, was observed for the prepared nanoparticles. Maximum TL sensitivity was found at 0.4 mol% of Ce impurity. Other TL dosimetry features, including reusability and fading, were also presented and discussed
tags: Nanoparticles Hydrothermal method Thermoluminescence CaF2:Ce