Effective preparation of amine-functionalized nano magnetite as a precursor of novel solid acid catalyst for one-pot synthesis of xanthenes under solvent-free conditions

نویسندگانحسین نعیمی,زهرا انصاریان
نشریهJ TAIWAN INST CHEM E
شماره صفحات265
شماره مجلد85
ضریب تاثیر (IF)3.849
نوع مقالهFull Paper
تاریخ انتشار2018-03-11
رتبه نشریهعلمی - پژوهشی
نوع نشریهالکترونیکی
کشور محل چاپایران
نمایه نشریهISI

چکیده مقاله

In this work, a facile route was developed for the preparation of amine-functionalized magnetite nanopar- ticles by co-precipitation method. These amine-functionalized magnetite nanoparticles were sulfonated and then used as novel heterogeneous acid catalyst and their catalytic activities were investigated in the green synthesis of 14-aryl-14H-dibenzo[a,j]xanthenes under thermal and solvent free conditions. The cat- alyst was characterized by FT-IR, SEM, EDX, XRD, TGA and VSM. Also, the catalyst could be recovered easily and reused several times without any significant loss of its catalytic activity.

tags: Nano-magnetite Synthesis Xanthenes Solvent-free Heterogeneous