Microwave-assisted practical and simple method for heterocyclization of o-phenylenediamine and aldehydes using DDQ as oxidant agent

نویسندگانحسین نعیمی,زهرا بابایی قریشوند
شماره صفحات129
شماره مجلد10
ضریب تاثیر (IF)1.729
نوع مقالهFull Paper
تاریخ انتشار2017-04-11
رتبه نشریهعلمی - پژوهشی
نوع نشریهالکترونیکی
کشور محل چاپایران
نمایه نشریهISI ,SCOPUS

چکیده مقاله

In this research, 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) has been used in the condensation reaction between o-phenylenediamine and various arylaldehydes as oxidants under microwave irradiation. In this clean reaction, the benzimidazole derivatives were synthesized as benefit target products. The advantages to this procedure include high yields, easy work-up procedure, no chromatographic separation, and short reaction times. The obtained pure products were characterized by physical and spectral data such as IR, 1H NMR and 13C NMR techniques.

tags: O-Phenylenediamine, benzimidazole, DDQ, aldehyde, microwave